Synthetic detergents, which are also known as
syndets, were developed to overcome the difficulties
faced while using soap as a cleaning agent. Soaps
when used in hard water precipitate the calcium
and magnesium salts, due to which it's effectiveness
as a cleaning agent deteriorates.
In addition, edible oil & fats, which could
be put to other uses, are used as raw materials
for the manufacture of soaps. These problems are
circumvented in synthetic detergents that are
highly stable in hard water and do not consume
valuable and expensive oil for their manufacture.
Detergent
Slurry Formulation
Detergent powder falls
into four major groups :
Heavy
duty detergents (high and low
foaming)
Light duty detergents
Soap
powders
Soda
products.
Detergent formulations
essentially consists of :
Active
ingredients
STPP
Filler
(e.g. Sodium sulphate)
Silicate
Normally active ingredients
used for detergents are linear alkyl benzyl sulphonates.
Detergent Spray
Drying
Free flowing, non dusty, non caking
detergent products in bead form are
produced by Spray Drying mostly in
counter current flow using pressure
nozzle atomization.
Inlet temperatures vary according
to product and upto 400°C inlet
temperatures are used for some detergents.
Hot air from direct fired air heaters
is used for Spray Drying. Exhaust
high efficiency cyclones / bag houses
are used to control emissions and
maximize product recovery are part
of the spray drying plant. RAJ offers
stand alone spray drying plants on
turnkey basis.
Pneumatic Conveying, Perfuming
& Packing
The dried detergent powder is pneumatically
conveyed from the Spray Dryer to the
product silos after sieving. Here
filtered atmospheric air is used as
the cooling & conveying media.
Dense phase conveying systems are
normally preferred.
The detergent product from the silo
is then blended along with the perfume
in a continuous mixer after which
it is packed.
Applications
Washing
Powders
(Detergents, Soaps, Surface Active Agents)
The free-flowing, non-dusty, non-caking
products in bead form are produced in counter-current
flow dryers with nozzle atomization is the
preferred layout for high-bulk-density detergents.
Feeds are homogenized and fine-filtered
prior to passing to nozzles operating at
high pressure. Hot air from direct-fired
air heaters enters at the base of the cylindrical
part of the tower with slight rotary motion.
The exhaust air is drawn from the top of
the tower. Inlet temperatures vary according
to product. Up to 400°C (750°F)
is used for some detergents, but lower temperatures
are used for fine washing agents. Product
recovery from the drying tower is high (99%).
The fines fraction is usually returned to
feed preparation. Open - cycle dryers are
normally used, Co-current dryers are used
for low - bulk - density detergents.
Soda Products
Detergent formulations consist basically
of (a) an active ingredient (b) sodium tripolyphosphate,
(c) silicates, (d) sodium sulphate. Normally
the active ingredients are fatty alcohol
sulphates, primary and secondary alkyl sulphonates
and alkyl aryl sulphonates. Synthetic detergents
are currently based upon linear alkyl benzene
sulphonates. Formulations are with variations
as decided by each company.
Heavy - Duty Detergents
Synthetic detergents are widely used in
cleaning of all types and operate successfully
with hard water. The coarse powder granules
in bead form are free-flowing, non-dusty
and readily dissolve in water. Shelf-life
is excellent, with no tendency to instability
or lumping. The feed can be formulated batchwise
or continuously. RAJ slurry preparation
systems ensures the right preparation technique
which improves the quality of the final
dried detergent powder. Precise weighing
/ metering, mixing, homogenizing and de-aeration
take place before spray drying. As high
a solid content as possible is used (50
- 65%) to give the optimum powder bulk density
and best economic use of the spray dryer.
The product is dried in a counter-current-flow
drying tower at inlet temperature 350 -
400°C (660 - 750°F). The dried powder
leaves the base of the drying tower and
is transported via a conveyor belt to an
air lift. During passage on the belt, product
dosing is carried out. Dosing materials
can be products that would be damaged during
spray drying, e.g. lauryl alcohol, enzymes.
Bleach alongwith enzymes is also added at
this stage. Perfume is added after the following
air lift.
Light Duty Detergents
Light - duty detergents are used less than
heavy duty. They find wide application only
in dish washing and light household cleaning
(janitoring). Light -duty detergents are
produced in nozzle towers with either co-current
or counter-current flow. Choice depends
upon required bulk density. Inlet drying
temperatures are also lower, 250 - 275°C
(480 - 530°F).
Detergent Allied Products
RAJ also provides state of art powder technology
for detergent allied products like Sodium
Lauryl Sulphate (SLS), Alfa Olefin Sulphonate
(AOS), Optical Brightening Agents (OBA),
Linear Alkyl Benzyl Sulphonate (LABSA),
Sodium Silicate, Sodium Tri-polyphosphate
(STPP).
Raj
Process Equipments And Systems Pvt. Ltd. is one of the
most specialized manufacturers of Detergent Plant Spray
Drying and Dryes & Pigments Spray Drying in India.